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A suggested sequence for pumping the cryo chamber is as
follows:
- IMPORTANT!
Make sure that the convectron controller located on the
cart under the air table (which is the one for the piezo interlock)
is connected to the convectron gauge at the upstream (front)
wall of the chamber. Otherwise the piezo may be under
high voltage in low vaccum, which would cause sparking.
- Inspect every flange. Especially look at the bellows at the
airlock and underneath the chamber -- are
they all ready to feel vacuum force?
- Make sure the turbo is vented, and the chamber is at
atmospheric pressure.
- Make sure all up-to-air valves (green and black handles,
Valves D and E) on prepump
line and vacuum chamber are closed.
- Open the valve between turbo and chamber by
flipping the ``Turbo Valve override'' switch on the cryo
interlock
front panel and pushing the ``open'' button. Start the turbo.
If it is a slow pumpdown, the turbo may
shut itself off after five minutes or so. If that happens,
just turn it right back on.
- At
torr, or when the turbo has reached 50% of its
maximum speed, you can switch off the override for the turbo
valve. This will ensure that the interlock closes the valve in
case of (accidental) venting of the chamber. Also, the beamline
valves will not be allowed to open as long as a valve override
on the cryo interlock panel is on.
- With the turbo, you will be able to pump into the low
torr
range. For imaging, you may then want to
open the ion pump. NOTE: The ion pump should always be pumping on
itself when it is not pumping the chamber, therefore it should not
be turned off but instead be isolated from the chamber by closing
the gate valve.
The gate valve to the ion pump can be opened by pushing the
``Ion Pump Valve open'' button on the cryo interlock. To
protect the ion pump from high pressures, the gate valve will be
closed by the cryo interlock when the chamber pressure rises
above
torr.
- If you choose to use the ion pump, you can close the
electrically-controlled valve
to the turbo. Turn the turbo off so it vents itself. (If the cryo
chamber pressure rises during any of these steps, immediately
turn the turbo back on).
Next: Sample Transfer
Up: Vacuum procedures
Previous: Venting the cryo chamber
  Contents
Tobias Beetz
2001-04-23