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Here are the instructions, but I recommend using the STXM IV instead!
The cryo interlock will allow the chamber to be filled with up to
torr of air or any gas. Here is how to proceed:
- Make sure you are aligned since the piezos will be disabled when
the pressure rises above 1 mtorr.
- Close V9i, to protect the beamline (just in case - the interlock
should take care of accidents anyway).
- Close the valve between turbo and chamber by pushing the ``Turbo
valve close'' button on the cryo interlock control panel.
Leave the turbo running.
- While watching the chamber convectron gauge, slowly open the
chamber venting valve on the outboard side of the chamber (black
handle). Close the valve as soon as you've reached the desired
pressure.
- Open V9i; now you can take all the spectra you want.
- If you are done and you want to pump the chamber back down,
open the Turbo valve on the cryo interlock control panel.
Check that the turbo keeps spinning at full speed. If not,
turn it off and right back on, and the chamber should pump
down fine.
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Tobias Beetz
2001-04-23